Contact an Account ManagerDetection of oxilofrine in plasma and urine by HPLC with electrochemical detection and comparison with gas chromatography - mass spectrometry
Summary
Type: HPLC
Application #: 102970
Catalog#: 720120.46 - MN HPLC Column, Nucleosil C18, 100A, 5um, 4.6x150mm
Detection: electrochemical, 0.95V versus Ag/AgCl
Conditions: eluent: 0.05M Na acetate, 50mg/l EDTA and 100mg/ml heptanesulphonic acid, adjusted to pH 4.5 with acetic acid - methanol (87.5 : 12.5, v/v)
flow rate 1.0ml/min
Authors: Kauert G
Source: J Chromatogr 428 (1988) 291 - 300
Details
Legend: Fig. 3. Chromatograms of a volunteer's urine extract: a) without oxilofrine and
b) with 6.6µg/ml oxilofrine. Retention time of etilefrine (int. std.) is
9.36min.